Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside
CAS No.:155194-59-5
Molecular Formula:C₂₅H₂₇NO₇
Molecular Weight:453.492
Hs Code.:

Synonyms:Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

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Technology Process of Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

There total 1 articles about Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76101-14-9
methyl-2-desoxy-2-phthalimido-β-D-glucopyranoside

: 155194-59-5
Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / p-toluenesulfonic acid / acetone / 2 h

2: 75 percent / NaH / tetrahydrofuran / 1 h / Heating

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; acetone;

Reference yield: 99.0%

: 155194-59-5
Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

: 97242-85-8
methyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With acetic acid; at 50 ℃; for 2h;

Reference yield:

: 155194-59-5
Methyl 3-O-benzyl-2-deoxy-4,6-O-isopropylidene-2-phthalimido-β-D-glucopyranoside

: Methyl 4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-6-O-<4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl>-3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / aq. 50percent acetic acid / 2 h / 50 °C

2: 66 percent / BF₃*Et₂O, molecular sieves 4A / CH₂Cl₂

3: 64 percent / BF₃*Et₂O / CH₂Cl₂ / Ambient temperature

With 4 A molecular sieve; boron trifluoride diethyl etherate; acetic acid; In dichloromethane;