3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

Base Information

Chemical Name:3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate
CAS No.:347307-90-8
Molecular Formula:C₇₁H₆₂O₂₄
Molecular Weight:1299.26
Hs Code.:

Synonyms:3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

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Chemical Property of 3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

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Technology Process of 3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

There total 6 articles about 3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 186605-76-5
3,5-bis[3,5-bis(methoxycarbonyl)phenoxymethyl]phenol

: 347307-84-0
3,5-bis(bromomethyl)phenyl benzoate

: 347307-90-8
3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 41h; Heating;
DOI:10.1016/S0040-4020(01)00198-3

Reference yield:

: 5554-28-9
(3,5-Dimethylphenyl)benzoat

: 347307-90-8
3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 36 percent / NBS; tert-butylperoxide / CCl₄ / 24 h / Heating; illumination

2: 89 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

3: 94 percent / sodium methoxide / benzene; methanol / 0.5 h / Heating

4: 73 percent / K₂CO₃; 18-crown-6 / acetone / 41 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; di-tert-butyl peroxide; sodium methylate; potassium carbonate; In methanol; tetrachloromethane; acetone; benzene;
DOI:10.1016/S0040-4020(01)00198-3

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 347307-90-8
3,5-bis-[3,5-3,5-(dimethoxycarbonylphenoxymethyl)phenoxymethyl]phenyl benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / pyridine / 3 h / 20 °C

2: 36 percent / NBS; tert-butylperoxide / CCl₄ / 24 h / Heating; illumination

3: 89 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

4: 94 percent / sodium methoxide / benzene; methanol / 0.5 h / Heating

5: 73 percent / K₂CO₃; 18-crown-6 / acetone / 41 h / Heating

With pyridine; N-Bromosuccinimide; 18-crown-6 ether; di-tert-butyl peroxide; sodium methylate; potassium carbonate; In methanol; tetrachloromethane; acetone; benzene;
DOI:10.1016/S0040-4020(01)00198-3