7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Base Information

Chemical Name:7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione
CAS No.:1263869-30-2
Molecular Formula:C₁₃H₁₁ClN₂O₂
Molecular Weight:262.696
Hs Code.:

Synonyms:7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

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Technology Process of 7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

There total 5 articles about 7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1263869-29-9
7-(4-chlorophenyl)-6,7-dihydrocyclopenta[e][1,3]oxazine-2,4(3H,5H)-dione

: 1263869-30-2
7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: With ammonium hydroxide; In water; at 100 ℃; for 6h; High-pressure vessel;

Reference yield:

: C₁₄H₁₃ClN₂OS

: 1263869-30-2
7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: With catalyst 001×7 strong acid ion exchange resin; In ethanol; water; at 80 - 90 ℃; for 10h;

Reference yield:

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 1263869-30-2
7-(4-chlorophenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2 h / Reflux

1.2: Cooling with ice

2.1: formic acid; dihydrogen peroxide / 20 - 50 °C

3.1: 3 h / 58 - 130 °C

4.1: ammonium hydroxide / 6 h / 100 °C

With ammonium hydroxide; formic acid; dihydrogen peroxide;