5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

Base Information

Chemical Name:5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)
CAS No.:377733-54-5
Molecular Formula:C₆₂H₇₂CuN₄
Molecular Weight:936.826
Hs Code.:

Synonyms:5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

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Chemical Property of 5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

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Technology Process of 5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

There total 1 articles about 5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine

: 142-71-2
copper diacetate

: 377733-54-5
5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

Guidance literature:: In methanol; dichloromethane; CH2Cl2 soln. of porphyrin was added to a satd. soln. of Cu-acetate in MeOH, soln. was refluxed for 2 h; soln. was chromd. on silica gel, recrystn. from CH2Cl2 and MeOH;
DOI:10.1021/jp000306s

Reference yield: 25.0%

: 377733-54-5
5,10,15-tri(3,5-di-tert-butylphenyl)-21H,23H-porphine copper(II)

: 331991-38-9
(Cu(C(C₆H₃(C(CH₃)3)2)CCHCHCNCCCCHCNC(C₆H₃(C(CH₃)3)2)CCHCHCNC(C₆H₃(C(CH₃)3)2)CCHCHCN))2

: (Cu(C(C₆H₃(C(CH₃)3)2)CCHCHCNCCCHCHCNC(C₆H₃(C(CH₃)3)2)CCHCHCNC(C₆H₃(C(CH₃)3)2)CCHCHCN))2

: 377733-57-8
Cu(5,10,15-tri(3,5-di-tert-butylphenyl)-20-chloroporphyrin)

Guidance literature:: With (BrC₆H₄)3HNSbCl₆; In chloroform; Cu complex was oxidized by the hexachloroantimonate for 12 h at 25°C; the products were sepd. by SEC and then by chromy. (silica gel, hexane/CH2Cl2);
DOI:10.1021/ja0110933