(+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

Base Information

Chemical Name:(+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one
CAS No.:283594-59-2
Molecular Formula:C₁₅H₂₂N₂O₃S
Molecular Weight:310.417
Hs Code.:

Synonyms:(+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

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Chemical Property of (+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

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Technology Process of (+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

There total 2 articles about (+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₁₅H₂₂N₂O₃S

: 283594-59-2
(+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 - 22 ℃;
DOI:10.1016/S0040-4039(00)00307-5

Reference yield:

: 283594-53-6
(-)-(Z)-(3S,4R)-1-[(S)-N-methyl-S-phenylsulfonimidoyl]-4-methylhex-5-en-3-ol

: 3019-71-4
Trichloroacetyl isocyanate

: 283594-59-2
(+)-(4S,5R,6S)-tetrahydro-6-ethyl-5-methyl-4-{[(S)-N-methyl-S-phenylsulfonimidoyl]methyl}-2H-1,3-oxazin-2-one

Guidance literature:: (-)-(Z)-(3S,4R)-1-[(S)-N-methyl-S-phenylsulfonimidoyl]-4-methylhex-5-en-3-ol; Trichloroacetyl isocyanate; In tetrahydrofuran; at 20 ℃; for 2h;

With ammonium hydroxide; at 20 ℃; for 1h;

With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 18h;
DOI:10.1002/ejoc.200390210