thallium 2,3-dichlorophenylcyanamidate

Base Information

Chemical Name:thallium 2,3-dichlorophenylcyanamidate
CAS No.:120204-98-0
Molecular Formula:C₇H₃Cl₂N₂*Tl
Molecular Weight:390.403
Hs Code.:

Synonyms:thallium 2,3-dichlorophenylcyanamidate

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Chemical Property of thallium 2,3-dichlorophenylcyanamidate

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Technology Process of thallium 2,3-dichlorophenylcyanamidate

There total 1 articles about thallium 2,3-dichlorophenylcyanamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 71232-27-4
(2,3-dichlorophenyl)cyanamide

: 563-68-8
thallium(I) acetate

: 120204-98-0
thallium 2,3-dichlorophenylcyanamidate

Guidance literature:: With triethylamine; In water; acetone; addn. of triethylamine to boiling 50/50 acetone/water soln. of 2,3-Cl2Hpcyd and TlAc, further boiling for 1 min; crystn. on cooling to room temp., washing (water, acetone), air-drying;

Reference yield: 72.0%

: cis-dichloro(2,2′-bipyridine)ruthenium(II)chloride

: 120204-98-0
thallium 2,3-dichlorophenylcyanamidate

: cis-bis(2,2'-bipyridine)bis((2,3-dichlorophenyl)cyanamido)ruthenium(II)

Guidance literature:: In N,N-dimethyl-formamide; byproducts: TlCl; 2 equiv. of Tl-salt, refluxing and stirring (3 h); cooling (refrigerator, overnight), filtration off TlCl, Et2O addn. (pptn. on cooling in refrigerator overnight), washing (ether), crystn. on ether diffusion into DMF soln.); elem. anal.;

Reference yield: 70.0%

: 120204-98-0
thallium 2,3-dichlorophenylcyanamidate

: 469867-80-9
cis-bis(2,2'-biryridine)carbonatocobalt(III) hexafluorophosphate

: cis-bis(2,5-dichlorophenylcyanamide)bis(2,2'-bipyridine)cobalt(III) hexafluorophosphate

Guidance literature:: In acetonitrile; byproducts: Tl2CO3; the mixt. in acetonitrile was stirred at reflux overnight, allowed to cool to room temp., left in refrigerator overnight; Tl2CO3 was filtered off, ether was added to filtrate, placed to refrigerator overnight, ppt. was fltered, washed with ether, recrystd. by diffusing ether into an acetonitrile soln.; elem. anal.;
DOI:10.1016/S0020-1693(02)00837-X