Technology Process of 4-(bromoethynyl)benzaldehyde oxime
There total 3 articles about 4-(bromoethynyl)benzaldehyde oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium hydroxide;
In
methanol;
for 0.15h;
Green chemistry;
DOI:10.1039/c2cc36315a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 26 h / 20 - 65 °C / Inert atmosphere; Green chemistry
2.1: potassium carbonate / methanol / 1 h / 20 °C / Green chemistry
3.1: silver nitrate / acetone / 0.5 h / Green chemistry
3.2: 72 h / Green chemistry
4.1: hydroxylamine hydrochloride; sodium hydroxide / methanol / 0.15 h / Green chemistry
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydroxylamine hydrochloride; potassium carbonate; silver nitrate; triethylamine; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol; acetone;
DOI:10.1039/c2cc36315a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / methanol / 1 h / 20 °C / Green chemistry
2.1: silver nitrate / acetone / 0.5 h / Green chemistry
2.2: 72 h / Green chemistry
3.1: hydroxylamine hydrochloride; sodium hydroxide / methanol / 0.15 h / Green chemistry
With
hydroxylamine hydrochloride; potassium carbonate; silver nitrate; sodium hydroxide;
In
methanol; acetone;
DOI:10.1039/c2cc36315a
