2-Acetylamino-6-bromobenzoic acid

Base Information

Chemical Name:2-Acetylamino-6-bromobenzoic acid
CAS No.:38792-45-9
Molecular Formula:C₉H₈BrNO₃
Molecular Weight:258.071
Hs Code.:
DSSTox Substance ID:DTXSID401294484
Nikkaji Number:J1.262.636C

Synonyms:38792-45-9;2-bromo-6-acetamidobenzoic acid;2-Acetylamino-6-bromobenzoic acid;DTXSID401294484;2-(Acetylamino)-6-bromobenzoic acid;EN300-28280408

Suppliers and Price of 2-Acetylamino-6-bromobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Acetylamino-6-bromobenzoic acid

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:256.96876
Heavy Atom Count:14
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=C(C(=CC=C1)Br)C(=O)O

Technology Process of 2-Acetylamino-6-bromobenzoic acid

There total 4 articles about 2-Acetylamino-6-bromobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 67866-91-5
N-(3-bromo-2-methylphenyl)acetamide

: 38792-45-9
2-acetamido-6-bromobenzoic acid

Guidance literature:: With potassium permanganate; magnesium sulfate; In water; for 2h; Heating;
DOI:10.1071/CH99135

Reference yield:

: 55289-36-6
3-bromo-2-methylaniline

: 38792-45-9
2-acetamido-6-bromobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 0.17 h

2: 73 percent / MgSO₄*7H₂O; KMnO₄ / H₂O / 2 h / Heating

With potassium permanganate; magnesium sulfate; In water; 1: Acetylation / 2: Oxidation;
DOI:10.1071/CH99135

Reference yield:

2-bromo-6-nitrotoluene: 55289-35-5
2-bromo-6-nitrotoluene

: 38792-45-9
2-acetamido-6-bromobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / stannous chloride dihydrate / ethanol / Heating

2: 77 percent / 0.17 h

3: 73 percent / MgSO₄*7H₂O; KMnO₄ / H₂O / 2 h / Heating

With potassium permanganate; magnesium sulfate; tin(ll) chloride; In ethanol; water; 1: Reduction / 2: Acetylation / 3: Oxidation;
DOI:10.1071/CH99135