2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione

Base Information

• Chemical Name: 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione
• CAS No.: 912999-91-8
• Molecular Formula: C₂₁H₂₃NO₆
• Molecular Weight: 385.417

Synonyms:2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione

Chemical Property of 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione

Chemical Property:

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Technology Process of 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione

There total 1 articles about 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-hydroxy-2-(4-methoxybenzyl)-1H-isoindole-1,3(2H)-dione (491875-13-9) + 2-bromoethyl 2-methoxyethyl ether (54149-17-6,92450-98-1) → 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione (912999-91-8)

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 43.5h;

Reference yield: 97.0%

2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-isoindole-1,3-dione (912999-91-8) → 2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-2,3-dihydro-1H-isoindole (912999-95-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 - 60 ℃; for 23h;

upstream raw materials:

4-hydroxy-2-(4-methoxybenzyl)-1H-isoindole-1,3(2H)-dione

2-bromoethyl 2-methoxyethyl ether

Downstream raw materials:

2-(4-methoxy-benzyl)-4-[2-(2-methoxy-ethoxy)-ethoxy]-2,3-dihydro-1H-isoindole

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