(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

Base Information

Chemical Name:(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon
CAS No.:50281-41-9
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

Suppliers and Price of (3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

There total 1 articles about (3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38274-02-1,50281-40-8,50281-41-9,51795-22-3,51795-23-4,54165-56-9,54165-57-0
Acetic acid 1,5,5-trimethyl-6-((E)-3-oxo-but-1-enyl)-7-oxa-bicyclo[4.1.0]hept-3-yl ester

Guidance literature:: aus Alkohol X;
DOI:10.1016/S0040-4039(01)84863-2

Reference yield: 73.0%

: 50281-41-9
(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

: (3S,5S,6S)-3-acetoxy-5,6-dihydroxy-5,6-dihydro-β-ionon

Guidance literature:: With sulfuric acid; In tetrahydrofuran; water; at 44 ℃; for 7h;
DOI:10.1002/hlca.19840670804

Reference yield:

: 50281-41-9
(3S,5S,6S)-3-acetoxy-5,6-epoxy-5,6-dihydro-β-ionon

: 96193-07-6
2-<(3S,5S,6S)-3,5,6-trihydroxy-5,6-dihydro-β-ionyliden>acetaldehyd

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / NaH / hexane; tetrahydrofuran / 20 h / Ambient temperature

2: 36 percent / H₂SO₄ / acetonitrile; H₂O / 1.45 h / Ambient temperature

3: 85 percent / DIBAH / diethyl ether; hexane / 1.5 h / 0 °C

4: 78 percent / MnO₂ / ethyl acetate / 1 h / Ambient temperature

With manganese(IV) oxide; sulfuric acid; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; hexane; water; ethyl acetate; acetonitrile;
DOI:10.1002/hlca.19840670804