5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

Base Information

Chemical Name:5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol
CAS No.:1312673-41-8
Molecular Formula:C₃₅H₃₈FNO₆
Molecular Weight:587.688
Hs Code.:

Synonyms:5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

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Chemical Property of 5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

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Technology Process of 5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

There total 2 articles about 5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1312673-46-3
2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl

: 1312673-41-8
5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

Guidance literature:: With hydrogenchloride; In acetic acid; at 70 ℃; for 4h;
DOI:10.1002/ejoc.201001412

Reference yield:

: 2-[3-(benzyloxy)-4-isopropoxyphenethyl]-2'-(4-fluoro-3-nitrostyryl)-4-isopropoxy-4'-methoxybiphenyl

: 1312673-41-8
5-{2-[2'-(4-fluoro-3-nitrophenethyl)-4-isopropoxy-4'-methoxybiphenyl-2-yl]ethyl}-2-isopropoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1: Wilkinson's catalyst; hydrogen / tetrahydrofuran; tert-butyl alcohol / 20 °C

2: hydrogenchloride / acetic acid / 4 h / 70 °C

With hydrogenchloride; Wilkinson's catalyst; hydrogen; In tetrahydrofuran; acetic acid; tert-butyl alcohol;
DOI:10.1002/ejoc.201001412