DIMETHYL ENDOTHAL

Base Information

• Chemical Name: DIMETHYL ENDOTHAL
• CAS No.: 88941-22-4
• Molecular Formula: C₁₀H₁₄O₅
• Molecular Weight: 214.218
• Hs Code.: 2932999099
• Mol file: 88941-22-4.mol

Synonyms:ENDOTHAL-DIMETHYL;DIMETHYL ENDOTHAL;ENDO-DIMETHYL 7-OXABICYCLO(2.2.1)HEPTANE-2,3-DICARBOXYLATE

Chemical Property of DIMETHYL ENDOTHAL

Chemical Property:

• PSA: 61.83000
• LogP: 0.12600
• Storage Temp.: 0-6°C

Purity/Quality:

99% ^*data from raw suppliers

DIMETHYL ENDOTHAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIMETHYL ENDOTHAL

There total 6 articles about DIMETHYL ENDOTHAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-dimethyl-7-oxa-norbornane-2endo,3endo-dicarboxylic acid dimethyl ester (116245-73-9) → (+/-)-1,4-dimethyl-7-oxa-norbornane-2endo,3exo-dicarboxylic acid (88941-22-4,109282-27-1,109282-37-3,129783-69-3)

Guidance literature:

With potassium hydroxide;

Reference yield:

1,4-dimethyl-7-oxa-norbornane-2exo,3exo-dicarboxylic acid dimethyl ester (54087-16-0) → (+/-)-1,4-dimethyl-7-oxa-norbornane-2endo,3exo-dicarboxylic acid (88941-22-4,109282-27-1,109282-37-3,129783-69-3)

Guidance literature:

With potassium hydroxide;

Reference yield:

2,5-dimethylfuran (625-86-5) → (+/-)-1,4-dimethyl-7-oxa-norbornane-2endo,3exo-dicarboxylic acid (88941-22-4,109282-27-1,109282-37-3,129783-69-3)

Guidance literature:

Multi-step reaction with 4 steps

1: Hydrieren des Reaktionsprodukts an Palladium/Calciumcarbonat in Aethylacetat und Erwaermen mit methanol. Kalilauge

2: platinum; acetic acid / Hydrogenation

3: diethyl ether

4: methanol. KOH-solution

With potassium hydroxide; diethyl ether; acetic acid; platinum;

upstream raw materials:

1,4-dimethyl-7-oxa-norbornane-2endo,3endo-dicarboxylic acid dimethyl ester

1,4-dimethyl-7-oxa-norbornane-2exo,3exo-dicarboxylic acid dimethyl ester

2,5-dimethylfuran

(+/-)-(1S,2R,3S,4R)-3-(methoxycarbonyl)-1,4-dimethyl-7-oxabicyclo[2.2.1]heptane-2-carboxylic acid