N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride

Base Information

• Chemical Name: N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride
• CAS No.: 145118-31-6
• Molecular Formula: C₃₁H₄₅N₅O₆*ClH
• Molecular Weight: 620.189

Synonyms:N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride

Chemical Property of N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride

There total 5 articles about N-(L-Alanyl)-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.8%

N-2,N6-Bis<(benzyloxy)carbonyl>-L-lysyl>-N'--L-alanyl>hexane-1,6-diamine (145118-30-5) → N-(L-Alanyl)-N'-2,N6-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride (145118-31-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 0.666667h;

DOI:10.1002/hlca.19920750617

Reference yield:

4-nitrophenyl N2,N6-bis[(phenylmethoxy)carbonyl]-L-lysinate (21160-82-7) → N-(L-Alanyl)-N'-2,N6-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride (145118-31-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 94.9 percent / Et₃N / tetrahydrofuran / 40 h

2: 94.3 percent / HCl / dioxane / 0.67 h

3: 71.1 percent / Et₃N / tetrahydrofuran / 18 h

4: 95.8 percent / HCl / dioxane / 0.67 h

With hydrogenchloride; triethylamine; In tetrahydrofuran; 1,4-dioxane;

DOI:10.1002/hlca.19920750617

Reference yield:

N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride (65915-94-8) → N-(L-Alanyl)-N'-2,N6-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine Hydrochloride (145118-31-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 94.9 percent / Et₃N / tetrahydrofuran / 40 h

2: 94.3 percent / HCl / dioxane / 0.67 h

3: 71.1 percent / Et₃N / tetrahydrofuran / 18 h

4: 95.8 percent / HCl / dioxane / 0.67 h

With hydrogenchloride; triethylamine; In tetrahydrofuran; 1,4-dioxane;

DOI:10.1002/hlca.19920750617

upstream raw materials:

N-2,N⁶-Bis<(benzyloxy)carbonyl>-L-lysyl>-N'--L-alanyl>hexane-1,6-diamine

4-nitrophenyl N₂,N₆-bis[(phenylmethoxy)carbonyl]-L-lysinate

N-(tert-butoxycarbonyl)-1,6-diaminohexane hydrochloride

N-2,N⁶-Bis<(benzyloxy)carbonyl>-L-lysyl>-N'-<(tert-butyloxy)carbonyl>hexane-1,6-diamine

Downstream raw materials:

N-2,N⁶-Bis<(Benzyloxy)carbonyl>-L-lysyl>-N'--L-alanyl>hexane-1,6-diamine

N-2,N⁶-Bis<(benzyloxy)carbonyl>-L-lysyl-N'-acetyl>-L-alanyl>hexane-1,6-diamine

N-acetyl>-L-alanyl>-N'-2,N⁶-bis<(benzyloxy)carbonyl>-L-lysyl>hexane-1,6-diamine

N-2,N⁶-Bis<(benzyloxy)carbonyl>-L-lysyl>-N'--L-alanyl>hexane-1,6-diamine

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