octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

Base Information

Chemical Name:octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside
CAS No.:155301-04-5
Molecular Formula:C₅₅H₆₈O₁₀
Molecular Weight:889.139
Hs Code.:

Synonyms:octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

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Chemical Property of octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

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Technology Process of octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

There total 3 articles about octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 155301-03-4
Acetic acid (2R,3S,4R,5R,6R)-3-benzyloxy-2-benzyloxymethyl-6-octyloxy-5-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 155301-04-5
octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

Guidance literature:: With sodium methylate; In methanol; Yield given; Ambient temperature;
DOI:10.1016/0008-6215(94)84275-2

Reference yield:

: 33639-77-9
perbenzyl fucosyl bromide

: 155301-04-5
octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: a) tetraethylammonium bromide, 4A molecular sieves / CH₂Cl₂; dimethylformamide / Ambient temperature; a) overnight, b) 2 d

2: NaOMe / methanol / Ambient temperature

With 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(94)84275-2

Reference yield:

: 155301-02-3
octyl 3-O-acetyl-4,6-di-O-benzyl-β-D-gulopyranoside

: 155301-04-5
octyl 4,6-di-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-β-D-gulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: a) tetraethylammonium bromide, 4A molecular sieves / CH₂Cl₂; dimethylformamide / Ambient temperature; a) overnight, b) 2 d

2: NaOMe / methanol / Ambient temperature

With 4 A molecular sieve; tetraethylammonium bromide; sodium methylate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(94)84275-2