28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

Base Information

Chemical Name:28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)
CAS No.:1039373-82-4
Molecular Formula:C₉₆H₁₀₄O₂₄
Molecular Weight:1641.87
Hs Code.:

Synonyms:28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

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Chemical Property of 28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

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Technology Process of 28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

There total 1 articles about 28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1039373-79-9
28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(3,4-O-isopropylidene-2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-6-O-(tert-butyldimethylsilyl)-β-D-glucopyranoside)

: 1039373-82-4
28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/jo800669h

Reference yield: 43.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1039373-82-4
28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside)

: C₉₉H₁₀₆O₂₇

: C₉₉H₁₀₄O₂₈

Guidance literature:: 28-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)oleanate 3-O-(2-O-benzoyl-α-L-arabinopyranosyl-(1->3)-2,4-di-O-benzoyl-β-D-glucopyranoside); With sodium periodate; In tetrahydrofuran; water; at 50 - 60 ℃; for 2h;

With jones reagent; In acetone; at 20 ℃; for 6h;

diazomethane; In diethyl ether; ethyl acetate; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1021/jo800669h