3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one

Base Information

• Chemical Name: 3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one
• CAS No.: 949562-87-2
• Molecular Formula: C₁₉H₂₂O₄S
• Molecular Weight: 346.447

Synonyms:3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one

Chemical Property of 3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one

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Technology Process of 3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one

There total 1 articles about 3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C9H12O2 + 3-(phenylsulfanyl)-3,4-dihydrofuran-2-one (35998-30-2) → 3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one (949562-87-2)

Guidance literature:

3-(phenylsulfanyl)-3,4-dihydrofuran-2-one; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -50 ℃; for 1h;

C₉H₁₂O₂; In tetrahydrofuran; at -50 ℃; for 3h; Further stages.;

DOI:10.1016/j.tet.2007.07.025

Reference yield: 95.0%

3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one (949562-87-2) + acetic anhydride (108-24-7) → acetic acid 2-(2-methyl-6-oxocyclohex-1-enyl)-1-(2-oxo-3-phenylsulfanyl-3,4-dihydrofuran-3-yl)ethyl ester (949562-88-3)

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1016/j.tet.2007.07.025

Reference yield:

3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-3-phenylsulfanyl-3,4-dihydrofuran-2-one (949562-87-2) → C19H22O5S

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2007.07.025

upstream raw materials:

3-(phenylsulfanyl)-3,4-dihydrofuran-2-one

Downstream raw materials:

acetic acid 2-(2-methyl-6-oxocyclohex-1-enyl)-1-(2-oxo-3-phenylsulfanyl-3,4-dihydrofuran-3-yl)ethyl ester

3-[1-hydroxy-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-5H-furan-2-one

acetic acid 2-(2-methyl-6-oxocyclohex-1-enyl)-1-(2-oxo-2,5-dihydrofuran-3-yl)ethyl ester

3-[1-(tert-butyldimethylsilanyloxy)-2-(2-methyl-6-oxocyclohex-1-enyl)ethyl]-5H-furan-2-one

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