5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine

Base Information

• Chemical Name: 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine
• CAS No.: 796119-00-1
• Molecular Formula: C₁₁H₁₂Cl₂N₂O₃
• Molecular Weight: 291.134
• Mol file: 796119-00-1.mol

Synonyms:5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine

Chemical Property of 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine

There total 1 articles about 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

5-(3,3-dichloro-allyloxy)-2-methoxybenzonitrile (796121-06-7) → 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine (796119-00-1)

Guidance literature:

5-(3,3-dichloro-allyloxy)-2-methoxybenzonitrile; With hydroxylamine hydrochloride; potassium carbonate; In ethanol; Heating / reflux;

With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; water; at 20 ℃; for 0.166667h;

With ammonia; In ethanol; water; pH=8;

Reference yield: 5.0%

4-(5-trifluoromethyl-pyridin-2-yloxy)-butanoic acid ethyl ester (796119-02-3) + 5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine (796119-00-1) → 2-(3-{3-[5-(3,3-dichloro-allyloxy)-2-methoxy-phenyl]-[1,2,4]oxadiazol-5-yl}-propoxy)-5-trifluoromethyl-pyridine

Guidance literature:

5-(3,3-dichloro-allyloxy)-N-hydroxy-2-methoxy-benzamidine; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.333333h;

4-(5-trifluoromethyl-pyridin-2-yloxy)-butanoic acid ethyl ester; In tetrahydrofuran; for 1h; Heating / reflux;

upstream raw materials:

5-(3,3-dichloro-allyloxy)-2-methoxybenzonitrile