C₃₄H₅₂O₃Si₂

Base Information

Chemical Name:C₃₄H₅₂O₃Si₂
CAS No.:1138157-68-2
Molecular Formula:C₃₄H₅₂O₃Si₂
Molecular Weight:564.956
Hs Code.:

C<sub>34</sub>H<sub>52</sub>O<sub>3</sub>Si<sub>2</sub>

Synonyms:C₃₄H₅₂O₃Si₂

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Chemical Property of C₃₄H₅₂O₃Si₂

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Technology Process of C₃₄H₅₂O₃Si₂

There total 7 articles about C₃₄H₅₂O₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1138157-66-0
C₃₄H₅₃IO₃Si₂

: 1138157-68-2
C₃₄H₅₂O₃Si₂

Guidance literature:: With trifuran-2-yl-phosphane; palladium diacetate; triethylamine; In water; acetonitrile; at 80 ℃; diastereoselective reaction;
DOI:10.1016/j.tetlet.2008.12.105

Reference yield:

: 1138157-37-5
C₂₄H₃₄O₃Si

: 1138157-68-2
C₃₄H₅₂O₃Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: mercury(II) trifluoroacetate / Reflux

1.2: Reflux

2.1: n-butyllithium / tetrahydrofuran

3.1: Dess-Martin periodane

4.1: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / -78 °C

5.1: N-iodo-succinimide; silver nitrate / N,N-dimethyl-formamide / 20 °C

5.2: 20 °C

5.3: 20 °C

6.1: trifuran-2-yl-phosphane; palladium diacetate; triethylamine / water; acetonitrile / 80 °C

With N-iodo-succinimide; n-butyllithium; borane-THF; trifuran-2-yl-phosphane; palladium diacetate; mercury(II) trifluoroacetate; Dess-Martin periodane; silver nitrate; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Claisen rearrangement / 6.1: Intramolecular Heck reaction;
DOI:10.1016/j.tetlet.2008.12.105

Reference yield:

: C₂₆H₃₆O₃Si

: 1138157-68-2
C₃₄H₅₂O₃Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran

2.1: Dess-Martin periodane

3.1: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / -78 °C

4.1: N-iodo-succinimide; silver nitrate / N,N-dimethyl-formamide / 20 °C

4.2: 20 °C

4.3: 20 °C

5.1: trifuran-2-yl-phosphane; palladium diacetate; triethylamine / water; acetonitrile / 80 °C

With N-iodo-succinimide; n-butyllithium; borane-THF; trifuran-2-yl-phosphane; palladium diacetate; Dess-Martin periodane; silver nitrate; triethylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile; 5.1: Intramolecular Heck reaction;
DOI:10.1016/j.tetlet.2008.12.105