7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

Base Information

Chemical Name:7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine
CAS No.:95610-88-1
Molecular Formula:C₁₄H₁₄N₂O₄
Molecular Weight:274.276
Hs Code.:

Synonyms:7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

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Chemical Property of 7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

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Technology Process of 7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

There total 3 articles about 7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 94936-52-4
3-benzoyl-5-(methoxycarbonyl)-2,3,5-oxadiazabicyclo<2.2.2>oct-7-ene

: 95610-88-1
7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

Guidance literature:: at 25 ℃; for 360h;
DOI:10.1021/jo00212a015

Reference yield:

: 33707-36-7
1-(methoxycarbonyl)-1,2-dihydropyridine

: 95610-88-1
7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / tetraethylammonium periodate / CH₂Cl₂ / 6 h / -78 - 25 °C

2: 100 percent / 360 h / 25 °C

With tetraethylammonium metaperiodate; In dichloromethane;
DOI:10.1021/jo00212a015

Reference yield:

: 495-18-1
Benzohydroxamic acid

: 95610-88-1
7-(methoxycarbonyl)-3-phenyl-4a,7,8,8a-tetrahydropyrido<4,3-e>-1,4,2-dioxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / tetraethylammonium periodate / CH₂Cl₂ / 6 h / -78 - 25 °C

2: 100 percent / 360 h / 25 °C

With tetraethylammonium metaperiodate; In dichloromethane;
DOI:10.1021/jo00212a015