(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

Base Information

Chemical Name:(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine
CAS No.:1156547-01-1
Molecular Formula:C₃₂H₃₉Br₂NO₂
Molecular Weight:629.475
Hs Code.:

Synonyms:(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

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Chemical Property of (R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

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Technology Process of (R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

There total 1 articles about (R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 139253-13-7
2,2'-bis(bromomethyl)-3,3'-dibromo-4,4'-dimethoxy-5,5'-di-tert-butylbiphenyl

: 1156547-01-1
(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

Guidance literature:: With potassium carbonate; In chloroform; at 60 ℃; for 18h;
DOI:10.1055/s-0028-1087810

Reference yield: 92.0%

: 1156547-01-1
(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

: 192182-54-0
3,5-dimethoxyphenylboronic acid

: 1156547-04-4
C₄₈H₅₇NO₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium carbonate; In tetrahydrofuran; at 70 ℃;
DOI:10.1055/s-0028-1087810

Reference yield: 74.0%

: 1156547-01-1
(R)-4,8-dibromo-2,10-di-tert-butyl-3,9-dimethoxy-6-(1-phenylethyl)-6,7-dihydro-5H-dibenzo[c,e]azepine

: 143418-49-9
3,4,5-trifluorophenylboronic acid

: 1156547-06-6
C₄₄H₄₃F₆NO₂

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; at 150 ℃;
DOI:10.1055/s-0028-1087810