C₃₀H₂₄O₂S

Base Information

Chemical Name:C₃₀H₂₄O₂S
CAS No.:1446907-37-4
Molecular Formula:C₃₀H₂₄O₂S
Molecular Weight:448.585
Hs Code.:

C<sub>30</sub>H<sub>24</sub>O<sub>2</sub>S

Synonyms:C₃₀H₂₄O₂S

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Chemical Property of C₃₀H₂₄O₂S

Chemical Property:

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Technology Process of C₃₀H₂₄O₂S

There total 4 articles about C₃₀H₂₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1446907-34-1
C₄₈H₆₄O₂SSi₂

: 1446907-37-4
C₃₀H₂₄O₂S

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol401697d

Reference yield:

: 740810-54-2
2-ethynyl-5-[2-(triisopropylsilyl)ethynyl]thiophene

: 1446907-37-4
C₃₀H₂₄O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; copper(l) iodide; triphenylphosphine; diisopropylamine / 18 h / 75 °C / Inert atmosphere

2: copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; 1,4-diaza-bicyclo[2.2.2]octane / toluene / 18 h / 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; tetrabutyl ammonium fluoride; palladium diacetate; diisopropylamine; triphenylphosphine; In tetrahydrofuran; toluene; 1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ol401697d

Reference yield:

: 1446907-31-8
C₂₅H₃₁BrO₂SSi

: 1446907-37-4
C₃₀H₂₄O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; 1,4-diaza-bicyclo[2.2.2]octane / toluene / 18 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; tetrabutyl ammonium fluoride; In tetrahydrofuran; toluene; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol401697d