(3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C

Base Information

• Chemical Name: (3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C
• CAS No.: 165067-86-7
• Molecular Formula: C₁₄H₁₃NO₆
• Molecular Weight: 293.249

Synonyms:(3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C

Chemical Property of (3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C

Chemical Property:

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Technology Process of (3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C

There total 1 articles about (3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C₄-14C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3'R,4'S)-2-(cis-3'-acetoxy-2'-oxo-4'-phenylazetidin-1'-yl)but-2-enoic acid methyl ester-C4'-14C → (3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C4-14C (165067-86-7)

Guidance literature:

With dimethylsulfide; ozone; Yield given. Multistep reaction; 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, RT;

DOI:10.1002/jlcr.2580360512

Reference yield: 100.0%

(3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C4-14C (165067-86-7) → (3R,4S)-cis-3-hydroxy-4-phenylazetidin-2-one-C4-14C (165067-88-9)

Guidance literature:

With sodium hydrogencarbonate; sodium carbonate; In methanol; for 3.5h;

DOI:10.1002/jlcr.2580360512

Reference yield: 68.0%

(3R,4S)-(cis-3-acetoxy-2-oxo-4-phenylazetidin-1-yl)oxoacetic acid methyl ester-C4-14C (165067-86-7) → (3R,4S)-acetic acid cis-2-oxo-4-phenylazetidin-1-yl ester-C4-14C

Guidance literature:

With hydrazine hydrate; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1002/jlcr.2580360512

Downstream raw materials:

(3R,4S)-cis-3-hydroxy-4-phenylazetidin-2-one-C₄-14C

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