4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

Base Information

Chemical Name:4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide
CAS No.:1356472-35-9
Molecular Formula:C₃₅H₃₇BrO₈
Molecular Weight:665.578
Hs Code.:

Synonyms:4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

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Chemical Property of 4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

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Technology Process of 4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

There total 1 articles about 4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1356472-29-1
4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl alcohol

: 1356472-35-9
4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1039/c1nj20841a

Reference yield: 98.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1356472-35-9
4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

: 1356472-06-4
4-(4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)nitrobenzene

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 24h; Reflux;
DOI:10.1039/c1nj20841a

Reference yield:

: 1356472-35-9
4-(4-(4-(4-allyloxy-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyloxy)-3-methoxybenzyl bromide

: 93-51-6
2-Methoxy-4-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 24 h / Reflux

2: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; acetone; 1: Williamson etherification;
DOI:10.1039/c1nj20841a