1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

Base Information

Chemical Name:1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride
CAS No.:798565-73-8
Molecular Formula:C₂₁H₂₀N₂O₅*ClH
Molecular Weight:416.861
Hs Code.:

Synonyms:1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

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Chemical Property of 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

Chemical Property:

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Technology Process of 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

There total 6 articles about 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798565-62-5
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carbonitrile

: 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboximidic acid ethyl ester hydrochloride

: 798565-73-8
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 0 - 20 ℃; for 12h;

Reference yield:

: 798565-45-4
1-bromo-6,7-dimethoxyisoquinoline-4-carbonitrile

: 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboximidic acid ethyl ester hydrochloride

: 798565-73-8
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride; 1,3-dimethylimidazolim iodide / DMF (N,N-dimethyl-formamide) / 0.5 h

2: hydrogenchloride / ethanol / 12 h / 0 - 20 °C

With hydrogenchloride; sodium hydride; 1,3-dimethylimidazolim iodide; In DMF (N,N-dimethyl-formamide); ethanol;

Reference yield:

: 18029-59-9
ethyl (2-cyano-2-(3,4-dimethoxyphenyl)vinyl)carbamate

: 1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboximidic acid ethyl ester hydrochloride

: 798565-73-8
1-(3-ethoxy-benzoyl)-6,7-dimethoxy-isoquinoline-4-carboxylic acid amide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / diphenylether / 4 h / 230 °C

2: methoxybenzene; phosphorus(V) oxybromide / 1 h / 110 °C

3: sodium hydride; 1,3-dimethylimidazolim iodide / DMF (N,N-dimethyl-formamide) / 0.5 h

4: hydrogenchloride / ethanol / 12 h / 0 - 20 °C

With hydrogenchloride; sulfuric acid; sodium hydride; 1,3-dimethylimidazolim iodide; methoxybenzene; phosphorus(V) oxybromide; In DMF (N,N-dimethyl-formamide); diphenylether; ethanol;