4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

Base Information

Chemical Name:4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine
CAS No.:366496-56-2
Molecular Formula:C₃₄H₄₈N₆O₆
Molecular Weight:636.792
Hs Code.:

Synonyms:4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

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Chemical Property of 4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

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Technology Process of 4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

There total 4 articles about 4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 72460-28-7
2,2'-bipyridyl-4,4'-dicarboxylic acid chloride

: 180683-64-1
tert-butyl ((1S,2S)-2-aminocyclohexyl)carbamate

: 366496-56-2
4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h; Heating;
DOI:10.1039/b102180j

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 366496-56-2
4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dioxane / 22 h

2: 71 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C / Heating

With triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/b102180j

Reference yield:

: 6813-38-3
2,2'-Bipyridine-4,4'-dicarboxylic acid

: 366496-56-2
4,4'-bis(1-carbonyl-2-tert-butoxycarbonyl-S,S-1,2-diaminocyclohexyl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / thionyl chloride / 16 h / Heating

2: 71 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C / Heating

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1039/b102180j