6,7-epoxycitronellyl acetate

Base Information

• Chemical Name: 6,7-epoxycitronellyl acetate
• CAS No.: 1787-98-0
• Molecular Formula: C₁₂H₂₂O₃
• Molecular Weight: 214.305

Synonyms:6,7-epoxycitronellyl acetate

Chemical Property of 6,7-epoxycitronellyl acetate

Chemical Property:

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Technology Process of 6,7-epoxycitronellyl acetate

There total 1 articles about 6,7-epoxycitronellyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

6,7-epoxycitronellol (1564-98-3) + acetic anhydride (108-24-7) → 6,7-epoxycitronellyl acetate (1787-98-0)

Guidance literature:

In pyridine; at 20 ℃; for 6h;

DOI:10.1021/jo026506c

Reference yield: 81.7%

6,7-epoxycitronellyl acetate (1787-98-0) + thiophenol (108-98-5) → Acetic acid 7-hydroxy-3,7-dimethyl-6-phenylsulfanyl-octyl ester (91413-36-4)

Guidance literature:

Reference yield: 75.0%

(3S)-3,7-dimethyl-6,7-epoxyoctan-1-yl acetate (1787-98-0,73367-94-9,73367-95-0,130790-59-9) → (3S)-3-methyl-6-oxohexan-1-yl acetate (82426-10-6,84145-52-8)

Guidance literature:

With sodium periodate; periodic acid; In tetrahydrofuran; water; at 0 - 20 ℃; for 1.16667h;

DOI:10.1002/chem.202001356

upstream raw materials:

6,7-epoxycitronellol

acetic anhydride

Downstream raw materials:

Acetic acid 7-hydroxy-3,7-dimethyl-6-phenylsulfanyl-octyl ester

Acetic acid 6-benzenesulfinyl-7-hydroxy-3,7-dimethyl-octyl ester

(-)-3,7-dimethyl-6-phenylseleno-octane-1,7-diol

(3S)-3-methyl-6-oxohexan-1-yl acetate

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