5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

Base Information

Chemical Name:5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide
CAS No.:152576-13-1
Molecular Formula:C₁₆H₂₂N₂O₂SSi
Molecular Weight:334.514
Hs Code.:

Synonyms:5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

Chemical Property:

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Technology Process of 5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

There total 5 articles about 5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarboxamide

: 152576-13-1
5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

Guidance literature:: With Lawessons reagent; In toluene; for 5h; Heating;
DOI:10.1021/jm00076a018

Reference yield:

: 5368-81-0
methyl 3-methoxybenzoate

: 152576-13-1
5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

Guidance literature:: Multi-step reaction with 5 steps

1: 58 percent / DPPA, DBN / dimethylformamide / 18 h

2: 71 percent / NH₃ / dioxane / 16 h / 100 °C

3: 70 percent / BBr₃ / CH₂Cl₂ / 18 h / Ambient temperature

4: 70 percent / imidazole / dimethylformamide / Ambient temperature

5: 80 percent / Lawesson's reagent / toluene / 5 h / Heating

With Lawessons reagent; 1H-imidazole; 2,6-dichloro-benzonitrile; diphenyl-phosphinic acid; ammonia; boron tribromide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00076a018

Reference yield:

: 152576-12-0
5-(3-hydroxyphenyl)-4-oxazolecarboxamide

: 152576-13-1
5-<3-<(1,1-dimethylethyl)dimethylsilyloxy>phenyl>-4-oxazolecarbothiamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / imidazole / dimethylformamide / Ambient temperature

2: 80 percent / Lawesson's reagent / toluene / 5 h / Heating

With Lawessons reagent; 1H-imidazole; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00076a018