p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside
CAS No.:807361-00-8
Molecular Formula:C₆₁H₆₀O₁₁S
Molecular Weight:1001.21
Hs Code.:

Synonyms:p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

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Chemical Property of p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

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Technology Process of p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

There total 1 articles about p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 220645-55-6
p-methylphenyl 2-O-benzoyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 211678-08-9
p-methylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

: 807361-00-8
p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Guidance literature:: With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; In dichloromethane; at -70 - 20 ℃;
DOI:10.1016/j.tet.2005.02.023

Reference yield: 99.0%

: 807361-00-8
p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: C₅₄H₅₆O₁₁S

Guidance literature:: With sodium hydrogen sulfate; silica gel; In methanol; dichloromethane; at 20 ℃; for 10h;
DOI:10.1055/s-2007-984903

Reference yield: 42.0%

: 807361-23-5
p-tolyl 3,6-di-O-benzyl-2-deoxy-2-N-phthalimido-1-thio-β-D-glucopyranoside

: 807361-00-8
p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 809232-04-0
Benzyl-{3-[(2R,3R,4S,5R,6R)-3,4-bis-benzyloxy-6-benzyloxymethyl-5-((2S,3R,4S,5R,6R)-3,5-bis-benzyloxy-6-benzyloxymethyl-4-hydroxy-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-carbamic acid benzyl ester

: C₁₅₄H₁₅₄N₂O₃₀

Guidance literature:: p-tolyl 3,6-di-O-benzyl-2-deoxy-2-N-phthalimido-1-thio-β-D-glucopyranoside; p-methylphenyl 2-O-benzoyl-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; In dichloromethane; at -70 - 20 ℃;

Benzyl-{3-[(2R,3R,4S,5R,6R)-3,4-bis-benzyloxy-6-benzyloxymethyl-5-((2S,3R,4S,5R,6R)-3,5-bis-benzyloxy-6-benzyloxymethyl-4-hydroxy-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-carbamic acid benzyl ester; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; In dichloromethane; at -70 - 20 ℃;
DOI:10.1016/j.tet.2005.02.023