C₆₀H₇₈O₁₁

Base Information

Chemical Name:C₆₀H₇₈O₁₁
CAS No.:1264660-97-0
Molecular Formula:C₆₀H₇₈O₁₁
Molecular Weight:975.273
Hs Code.:

C<sub>60</sub>H<sub>78</sub>O<sub>11</sub>

Synonyms:C₆₀H₇₈O₁₁

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Chemical Property of C₆₀H₇₈O₁₁

Chemical Property:

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Technology Process of C₆₀H₇₈O₁₁

There total 28 articles about C₆₀H₇₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1264660-96-9
C₆₆H₉₂O₁₂Si

: 1264660-97-0
C₆₀H₇₈O₁₁

Guidance literature:: With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; stereoselective reaction;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-83-2
C₂₇H₂₇O₇P

: 1264660-97-0
C₆₀H₇₈O₁₁

Guidance literature:: Multi-step reaction with 15 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 0 °C

1.2: 1 h / 50 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

2.2: 0 - 20 °C

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

3.2: 2.5 h

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

6.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

7.2: 15 h

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

9.1: n-heptane; dichloromethane / -78 - 0 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

11.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

12.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

13.1: diethyl ether / -78 - 0 °C

14.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C

14.2: 0.33 h / -78 °C

15.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; triethylsilane; n-butyllithium; tetrapropylammonium perruthennate; trimethylsilyl trifluoromethanesulfonate; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 1.2: Suzuki-Miyaura coupling / 14.2: Aldol condensation;
DOI:10.1021/ol102925d

Reference yield:

: 1225339-89-8
C₄₃H₇₀O₈Si₂

: 1264660-97-0
C₆₀H₇₈O₁₁

Guidance literature:: Multi-step reaction with 13 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0 - 20 °C

1.2: 2.5 h

2.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 19 h / 20 °C / Molecular sieve

4.1: zinc trifluoromethanesulfonate / tetrahydrofuran / 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

5.2: 15 h

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C

7.1: n-heptane; dichloromethane / -78 - 0 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

9.1: 2,6-dimethylpyridine / dichloromethane / -78 °C

10.1: dimethyl sulfoxide / 3 h / 20 - 80 °C

11.1: diethyl ether / -78 - 0 °C

12.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / 0 °C

12.2: 0.33 h / -78 °C

13.1: triethylsilane; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 °C

With 1H-imidazole; 2,6-dimethylpyridine; triethylsilane; n-butyllithium; tetrapropylammonium perruthennate; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; sodium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; n-heptane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 12.2: Aldol condensation;
DOI:10.1021/ol102925d