6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside
CAS No.:1581698-71-6
Molecular Formula:C₃₂H₃₉N₃O₁₇
Molecular Weight:737.672
Hs Code.:

Synonyms:6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

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Chemical Property of 6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

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Technology Process of 6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

There total 1 articles about 6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1581698-69-2
6-O-benzoyl-α-D-glucopyranosyl-(1→3)-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside (di-6,6″-O-benzoylmelezitose)

: 1581698-71-6
6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With hydrogen azide; di-isopropyl azodicarboxylate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/bc500047r

Reference yield:

: 1581698-71-6
6-O-benzoyl-α-D-glucopyranosyl-(1→3)-6-O-azido-β-D-fructofuranoside 6-O-benzoyl-α-D-glucopyranoside

: 1581698-77-2
C₄₄H₆₀N₆O₁₆

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol; water / 1 h / 20 °C / Inert atmosphere

2: triethylphosphite copper(I) iodide complex / methanol; chloroform / 3 h / 100 °C / Sealed tube; Microwave irradiation

With triethylphosphite copper(I) iodide complex; potassium hydroxide; In methanol; chloroform; water; 2: |Huisgen Cycloaddition;
DOI:10.1021/bc500047r