C₄₀H₄₀N₂O₁₁

Base Information

• Chemical Name: C₄₀H₄₀N₂O₁₁
• CAS No.: 857467-69-7
• Molecular Formula: C₄₀H₄₀N₂O₁₁
• Molecular Weight: 724.764
• Mol file: 857467-69-7.mol

Synonyms:C₄₀H₄₀N₂O₁₁

Chemical Property of C₄₀H₄₀N₂O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₄₀N₂O₁₁

There total 1 articles about C₄₀H₄₀N₂O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2-azido-3,4,6-tri-O-benzoyl-2-deoxy-α-D-glucopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose (857465-88-4) → C40H40N2O11 (857467-69-7)

Guidance literature:

With palladium hydroxide on carbon; ammonium formate; In methanol; ethyl acetate; at 65 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.carres.2009.09.012

Reference yield:

C40H40N2O11 (857467-69-7) → 2-deoxy-2-sulfamino-α-D-glucopyranosyl-(1->4)-1,6-anhydro-2-deoxy-2-sulfamino-3-O-benzyl-β-D-glucopyranose disodium salt

Guidance literature:

C₄₀H₄₀N₂O₁₁; With triethylamine sulfur trioxide; sodium hydrogencarbonate; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 1h;

With sodium hydroxide; water;

Reference yield:

C40H40N2O11 (857467-69-7) → C40H38N2O17S2(2-)*2Na(1+)

Guidance literature:

With triethylamine sulfur trioxide; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

DOI:10.1016/j.carres.2009.09.012

upstream raw materials:

2-azido-3,4,6-tri-O-benzoyl-2-deoxy-α-D-glucopyranosyl-(1->4)-1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose