6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

Base Information

• Chemical Name: 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene
• CAS No.: 180136-86-1
• Molecular Formula: C₂₈H₃₀
• Molecular Weight: 366.546

Synonyms:6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

Chemical Property of 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

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Technology Process of 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

There total 2 articles about 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

6-tert-Butyl-16-((Z)-styryl)-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene (180136-95-2) → 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene (180136-86-1) + 16-((E)-2-Bromo-2-phenyl-vinyl)-6-tert-butyl-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene + 16-((Z)-2-Bromo-2-phenyl-vinyl)-6-tert-butyl-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene

Guidance literature:

With benzyltrimethylammonium tribromide; In dichloromethane; for 45h;

DOI:10.1021/jo9602433

Reference yield:

O,O-diethyl benzylphosphonate (1080-32-6) + 5-tert-butyl-8-formyl<2.2>metacyclophane → 6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene (180136-86-1)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, room temperature, 10 min, 2.) THF, hexane, 1h;

DOI:10.1021/jo9602433

Reference yield: 70.0%

6-tert-Butyl-16-((E)-styryl)-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene (180136-86-1) → 6-tert-Butyl-16-((Z)-styryl)-tricyclo[9.3.1.14,8]hexadeca-1(15),4,6,8(16),11,13-hexaene (180136-95-2)

Guidance literature:

In benzene; at 5 ℃; for 1h; Irradiation;

DOI:10.1021/jo9602433

upstream raw materials:

O,O-diethyl benzylphosphonate

6-tert-Butyl-16-((Z)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

Downstream raw materials:

6-tert-Butyl-16-((Z)-styryl)-tricyclo[9.3.1.1^4,8]hexadeca-1⁽¹⁵⁾,4,6,8⁽¹⁶⁾,11,13-hexaene

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