Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

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Chemical Name:Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester
CAS No.:122952-34-5
Molecular Formula:C₁₉H₂₅N₃O₃
Molecular Weight:343.426
Hs Code.:

Synonyms:Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

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Chemical Property of Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

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Technology Process of Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

There total 3 articles about Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 122952-32-3
C₁₉H₂₇N₃O₃

: 122952-34-5
Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In dichloromethane; at 20 ℃;
DOI:10.1021/jo00280a009

Reference yield:

: 122952-40-3
(E)-1-(benzoyloxy)-4-bromo-2-methyl-2-butene

: 122952-34-5
Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) dimsyl sodium

2: 90 percent / 1.) from 85 deg C to 130 deg C, 45 min, 2.) 130 deg C, 1 h

3: 30 percent / PdCl₂(CH₃CN)2 / CH₂Cl₂ / 20 °C

With dichloro bis(acetonitrile) palladium(II); sodium methylsulfinylmethanide; In dichloromethane;
DOI:10.1021/jo00280a009

Reference yield:

: 122952-30-1
Benzoic acid (E)-4-[cyano-(3-methyl-but-2-enyl)-amino]-2-methyl-but-2-enyl ester

: 122952-34-5
Benzoic acid (E)-4-(2-imino-3-methoxy-4,4-dimethyl-3,4-dihydro-2H-pyrimidin-1-yl)-2-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1.) from 85 deg C to 130 deg C, 45 min, 2.) 130 deg C, 1 h

2: 30 percent / PdCl₂(CH₃CN)2 / CH₂Cl₂ / 20 °C

With dichloro bis(acetonitrile) palladium(II); In dichloromethane;
DOI:10.1021/jo00280a009