5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole
CAS No.:861997-61-7
Molecular Formula:C₂₅H₄₀N₄S₃
Molecular Weight:492.817
Hs Code.:

5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1<i>H</i>-tetrazole

Synonyms:5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

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Technology Process of 5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

There total 7 articles about 5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 861997-60-6
7-(2-heptyl-[1,3]dithian-2-yl)-heptan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 861997-61-7
5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; for 0.166667h;
DOI:10.1021/jo0505270

Reference yield:

: 777891-09-5
tert-butyl-(7-iodo-heptyloxy)-diphenyl-silane

: 861997-61-7
5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: t-BuLi / tetrahydrofuran; pentane / 1 h / -78 °C

2: 1.22 g / TBAF / tetrahydrofuran / 1 h / 20 °C

3: 100 percent / PPh₃; diisopropyl azodicarboxylate / 0.17 h

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; tert.-butyl lithium; triphenylphosphine; In tetrahydrofuran; pentane;
DOI:10.1021/jo0505270

Reference yield:

: tert-butyl-[7-(2-heptyl-[1,3]dithian-2-yl)-heptyloxy]-diphenyl-silane

: 861997-61-7
5-[7-(2-heptyl-[1,3]dithian-2-yl)-heptylsulfanyl]-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.22 g / TBAF / tetrahydrofuran / 1 h / 20 °C

2: 100 percent / PPh₃; diisopropyl azodicarboxylate / 0.17 h

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/jo0505270