1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one

Base Information

• Chemical Name: 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one
• CAS No.: 62336-64-5
• Molecular Formula: C₂₉H₁₆N₂O₅
• Molecular Weight: 472.456

Synonyms:1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one

Chemical Property of 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one

Chemical Property:

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Technology Process of 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one

There total 2 articles about 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

1,3-bis-(4-nitrophenyl)-propan-2-one (15330-76-4) + 9,10-phenanthrenequinone (84-11-7) → 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one (62336-64-5)

Guidance literature:

With potassium hydroxide; In ethanol;

DOI:10.1021/jo00002a037

Reference yield:

4-nitrobenzeneacetic acid (104-03-0) → 1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one (62336-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 11.4 g / Ac₂O, NEt₃ / 1 h

2: 49 percent / KOH / ethanol

With potassium hydroxide; acetic anhydride; triethylamine; In ethanol;

DOI:10.1021/jo00002a037

Reference yield: 2.0%

1,3-bis(4-nitrophenyl)cyclopentaphenanthren-2-one (62336-64-5) + benzenediazonium-2-carboxylate hydrochloride (4661-46-5) → 9,14-bis(4-nitrophenyl)benzotriphenylene (131273-85-3)

Guidance literature:

With methyloxirane; In various solvent(s); for 5h; Heating;

DOI:10.1021/jo00002a037

upstream raw materials:

1,3-bis-(4-nitrophenyl)-propan-2-one

9,10-phenanthrenequinone

4-nitrobenzeneacetic acid

Downstream raw materials:

C₃₉H₂₂ClN₃O₇

C₃₉H₂₂BrN₃O₇

9,14-bis(4-nitrophenyl)benzotriphenylene

9,14-bis(4-nitrophenyl)-11-methylbenzotriphenylene

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