3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

Base Information

Chemical Name:3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol
CAS No.:176981-19-4
Molecular Formula:C₄₉H₅₁NO₆Si
Molecular Weight:778.033
Hs Code.:

3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

Synonyms:3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

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Chemical Property of 3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

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Technology Process of 3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

There total 1 articles about 3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 176981-18-3
[3-(tert-Butyl-diphenyl-silanyloxymethyl)-1,10-dimethoxy-9-phenylsulfanyl-6,7,8,9-tetrahydro-benzo[g]isoquinolin-9-yl]-(3,6-dimethoxy-2-phenylethynyl-phenyl)-methanol

: 176981-19-4
3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); triphenylstannane; In benzene; for 6h; Heating;
DOI:10.1016/0040-4020(96)00245-1

Reference yield: 85.0%

: 176981-19-4
3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

: 176981-20-7
3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-6',7',8',9'-tetrahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1(3H)-one

Guidance literature:: With Ph₃BiCO₃; In pyridine; toluene; at 80 ℃; for 4.5h;
DOI:10.1016/0040-4020(96)00245-1

Reference yield:

: 176981-19-4
3'-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-3-(phenylmethylene)-1,3,6',7',8',9'-hexahydro-1',4,7,10'-tetramethoxyspiro(2H-indene-2,9'-benz[g]isoquinolin)-1-ol

: 176981-21-8
C₄₉H₅₁NO₈Si

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Ph₃BiCO₃ / toluene; pyridine / 4.5 h / 80 °C

2: OsO₄ / pyridine / 4 h / Ambient temperature

With osmium(VIII) oxide; Ph₃BiCO₃; In pyridine; toluene;
DOI:10.1016/0040-4020(96)00245-1