bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

Base Information

Chemical Name:bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid
CAS No.:82240-33-3
Molecular Formula:C₂₆H₁₆N₈O₁₄
Molecular Weight:664.458
Hs Code.:

Synonyms:bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

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Chemical Property of bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

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Technology Process of bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

There total 3 articles about bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82240-30-0
dimethyl 2,6-bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>-adamantane-1,7-dicarboxylate

: 82240-33-3
bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

Guidance literature:: With potassium hydroxide; In diethylene glycol; at 180 - 200 ℃; for 6h;
DOI:10.1007/BF00503563

Reference yield:

: 53120-57-3
tetramethyl adamantane-2,6-dione-1,3,5,7-tetracarboxylate

: 82240-33-3
bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / 15percent H₂SO₄ / dioxane / 24 h / Ambient temperature

2: 80 percent / KOH / bis-(2-hydroxy-ethyl) ether / 6 h / 180 - 200 °C

With potassium hydroxide; sulfuric acid; In 1,4-dioxane; diethylene glycol;
DOI:10.1007/BF00503563

Reference yield:

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 82240-33-3
bis(2,4-dinitrophenylpyrazolone-5)-<1,2-b,e>adamantane-1,7-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / 15percent H₂SO₄ / dioxane / 24 h / Ambient temperature

2: 80 percent / KOH / bis-(2-hydroxy-ethyl) ether / 6 h / 180 - 200 °C

With potassium hydroxide; sulfuric acid; In 1,4-dioxane; diethylene glycol;
DOI:10.1007/BF00503563