ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

Base Information

Chemical Name:ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate
CAS No.:1403889-26-8
Molecular Formula:C₁₈H₁₅Cl₂N₃O₃
Molecular Weight:392.241
Hs Code.:

Synonyms:ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

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Technology Process of ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

There total 1 articles about ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70249-85-3
carbethoxyhydrazone du benzoate d'ethyle

: 1403889-26-8
ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: neat (no solvent) / 0.17 h / 185 °C / Microwave irradiation; Sealed tube

2.1: potassium carbonate / acetone / 0.08 h / 90 °C / Microwave irradiation; Sealed tube

2.2: 0.17 h / 90 °C / Microwave irradiation; Sealed tube

With potassium carbonate; In acetone;
DOI:10.3184/174751912X13400138806685

Reference yield: 89.0%

: 1403889-26-8
ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

: 1403889-30-4
2-[4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 130 ℃; for 0.166667h; Temperature; Time; Microwave irradiation; Sealed tube;
DOI:10.3184/174751912X13400138806685

Reference yield:

: 1403889-26-8
ethyl [4-(3,5-dichlorophenyl)-3-phenyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]acetate

: 1403889-34-8
4-(3,5-dichlorophenyl)-2-[(5-mercapto-1,3,4-oxadiazol-2-yl)methyl]-5-phenyl-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / ethanol / 0.17 h / 130 °C / Microwave irradiation; Sealed tube

2.1: potassium hydroxide / ethanol; water / 0.08 h / 100 °C / Microwave irradiation

2.2: 0.17 h / 100 °C / Microwave irradiation

With hydrazine hydrate; potassium hydroxide; In ethanol; water;
DOI:10.3184/174751912X13400138806685