C₁₃H₁₃NO

Base Information

Chemical Name:C₁₃H₁₃NO
CAS No.:1173167-31-1
Molecular Formula:C₁₃H₁₃NO
Molecular Weight:199.252
Hs Code.:

Synonyms:C₁₃H₁₃NO

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Chemical Property of C₁₃H₁₃NO

Chemical Property:

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Technology Process of C₁₃H₁₃NO

There total 4 articles about C₁₃H₁₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1142955-20-1
C₁₆H₂₁NOSi

: 1173167-31-1
C₁₃H₁₃NO

Guidance literature:: With water; potassium carbonate; In tetrahydrofuran; methanol; for 1h;
DOI:10.1021/jo200246q

Reference yield:

: 115599-48-9
2-(4-iodophenyl)-4,4-dimethyl-4,5-dihydrooxazole

: 1173167-31-1
C₁₃H₁₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 6 h / Inert atmosphere

2: water; potassium carbonate / tetrahydrofuran; methanol / 1 h

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; 1: Sonogashira coupling;
DOI:10.1021/jo200246q

Reference yield:

: 2-[N-(4-iodobenzoyl)amino]-2-methyl-1-propanol

: 1173167-31-1
C₁₃H₁₃NO

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 0.5 h / 25 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / tetrahydrofuran / 6 h / Inert atmosphere

3: water; potassium carbonate / tetrahydrofuran; methanol / 1 h

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; thionyl chloride; water; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; 2: Sonogashira coupling;
DOI:10.1021/jo200246q