η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Base Information

Chemical Name:η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride
CAS No.:100228-92-0
Molecular Formula:C₄₂H₄₁ClP₂PdSi
Molecular Weight:777.694
Hs Code.:

Synonyms:η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Suppliers and Price of η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

There total 3 articles about η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 203172-52-5
Pd((CH₃)3SiC₂CH₂)(Cl)(P(C₆H₅)3)

: 203172-58-1
(Pd((CH₃)3SiC₂CH₂)(Cl)(P(C₆H₅)3))2

: 603-35-0
triphenylphosphine

: 100228-92-0
η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Guidance literature:: In chloroform-d1; equimolar P-compd. addn. to Pd-complex in solvent; monitoring by (1)H-NMR spectroscopy;
DOI:10.1021/ja973383i

Reference yield:

: 172162-33-3
(μ-η3-Me3SiCCCH2)(μ-Cl)Pd2(triphenylphosphine)2

: 603-35-0
triphenylphosphine

: [(Pd(PPh₃)2)n]

: 100228-92-0
η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Guidance literature:: In not given; addn. of PPh3 to Pd complex;
DOI:10.1021/ja003754m

Reference yield:

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 18135-82-5
(3-chloro-1-propynyl)trimethylsilane

: 100228-92-0
η1-Me3SiCCCH2 bistriphenylphosphine palladium chloride

Guidance literature:: In tetrahydrofuran; alkyne was added at once to Pd(PPh3)4 in THF at 20°C under N2, mixt. was stirred for 15 min at 20°C; half the vol. of solvent was evapd. at reduced pressure, n-pentane added, ppt. was collected, washed with Et2O, pentane, dried in vacuo (20°C, 0.02 mm Hg, 3 h); elem. anal.;