methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

Base Information

Chemical Name:methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate
CAS No.:1094780-03-6
Molecular Formula:C₃₅H₃₈N₄O₆
Molecular Weight:610.71
Hs Code.:

Synonyms:methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

Suppliers and Price of methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

There total 1 articles about methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: C₂HF₃O₂*C₂₇H₃₂N₄O₅

: 1094780-03-6
methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

Guidance literature:: phenylacetic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

C₂HF₃O₂*C₂₇H₃₂N₄O₅; In dichloromethane; for 1h; pH=8;
DOI:10.1021/jm801205x

Reference yield: 81.0%

: 1094780-03-6
methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

: 1094780-05-8
(2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoic acid

Guidance literature:: With lithium hydroxide; water; In methanol; for 1.5h;
DOI:10.1021/jm801205x

Reference yield:

: 1094780-03-6
methyl (2S)-6-{[(benzyloxy)carbonyl]amino}-2-[(4R)-3-oxo-4-[(phenylacetyl)amino]-3,4,5,10-tetrahydroazepino[3,4-b]indol-2(1H)-yl]hexanoate

: C₂₇H₃₂N₄O₄*ClH

Guidance literature:: With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In ethanol; under 1034.32 - 2585.81 Torr; Autoclave;
DOI:10.1021/jm801205x