2-t-BuC₆H₄PCl₂

Base Information

• Chemical Name: 2-t-BuC₆H₄PCl₂
• CAS No.: 1237893-82-1
• Molecular Formula: C₁₀H₁₃Cl₂P
• Molecular Weight: 235.093

Synonyms:2-t-BuC₆H₄PCl₂

Chemical Property of 2-t-BuC₆H₄PCl₂

Chemical Property:

Purity/Quality:

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Technology Process of 2-t-BuC₆H₄PCl₂

There total 3 articles about 2-t-BuC₆H₄PCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-t-BuC6H4P(NEt2)2 → 2-t-BuC6H4PCl2 (1237893-82-1)

Guidance literature:

With hydrogenchloride; In dichloromethane; Inert atmosphere;

DOI:10.1002/hc.20606

Reference yield:

2-(1,1-dimethylethyl)-benzenamine (6310-21-0) → 2-t-BuC6H4PCl2 (1237893-82-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrogen bromide; sodium nitrite / Inert atmosphere

1.2: Inert atmosphere

2.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

2.2: 20 °C / Inert atmosphere

3.1: hydrogenchloride / dichloromethane / Inert atmosphere

With hydrogenchloride; hydrogen bromide; magnesium; sodium nitrite; In tetrahydrofuran; dichloromethane; 1.1: Sandmeyer reaction / 1.2: Sandmeyer reaction;

DOI:10.1002/hc.20619

Reference yield:

2-tert-butylbromobenzene (7073-99-6) → 2-t-BuC6H4PCl2 (1237893-82-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

1.2: 20 °C / Inert atmosphere

2.1: hydrogenchloride / dichloromethane / Inert atmosphere

With hydrogenchloride; magnesium; In tetrahydrofuran; dichloromethane;

DOI:10.1002/hc.20619

upstream raw materials:

2-tert-butylbromobenzene

2-(1,1-dimethylethyl)-benzenamine

Downstream raw materials:

2-i-PrC₆H₄PH₂

2-i-PrC₆H₄P(SiMe₃)2

2-t-BuC₆H₄P(SiMe₃)2

2-t-BuC₆H₄PH₂

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