N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine

Base Information

• Chemical Name: N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine
• CAS No.: 389117-85-5
• Molecular Formula: C₂₅H₄₂N₄O₁₄S
• Molecular Weight: 654.693

Synonyms:N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine

Chemical Property of N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine

Chemical Property:

Purity/Quality:

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Technology Process of N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine

There total 1 articles about N^α,N^ε-Bis-[(1s_n,3R,4s_n,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα,Nε-Bis-[(1sn,3R,4sn,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-[S-(tert-butylthio)]-L-cysteinyl-glycine → Nα,Nε-Bis-[(1sn,3R,4sn,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine (389117-85-5)

Guidance literature:

With tributylphosphine; water; In propan-1-ol; at 20 ℃; for 24h;

DOI:10.1039/a904679h

Reference yield: 66.0%

(ClCH2CO)-Lys(ClCH2CO)-Lys-β-Ala-NH2 + Nα,Nε-Bis-[(1sn,3R,4sn,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine (389117-85-5) → C68H114N14O33S2

Guidance literature:

With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1039/a904679h

Reference yield: 56.0%

Nα,Nε-Bis-[(1sn,3R,4sn,5R)-1,3,4,5-tetrahydroxycyclohexanecarbonyl]-L-lysyl-L-cysteinyl-glycine (389117-85-5) + [(ClCH2CO)-Lys(ClCH2CO)]2-Lys-Lys-β-Ala-NH2 (250358-50-0) → C135H224N26O65S4

Guidance literature:

With potassium carbonate; In water; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1039/a904679h

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