2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside
CAS No.:163152-19-0
Molecular Formula:C₃₁H₃₄ClNO₁₃
Molecular Weight:664.063
Hs Code.:

Synonyms:2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

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Chemical Property of 2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

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Technology Process of 2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

There total 5 articles about 2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 94-33-7
C₉H₁₀O₃

: 163152-13-4
1,3,4,6-tetra-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranose

: 163152-19-0
2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 3 A molecular sieve; iron(III) chloride; In dichloromethane; for 48h; Ambient temperature;

Reference yield:

: 612-20-4
2-(hydroxymethyl)benzoic acid

: 163152-19-0
2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / 2-methoxypyridine / dimethylformamide / 1 h

2: 96 percent / thionyl chloride / 24 h / Ambient temperature

3: 71 percent / pyridine / CH₂Cl₂ / 16 h / Ambient temperature

4: 55 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 48 h / Ambient temperature

With pyridine; 2-methoxypyridine; thionyl chloride; 3 A molecular sieve; iron(III) chloride; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 163152-19-0
2-benzoyloxyethyl 3,4,6-tri-O-acetyl-2-<2-(chloroacetoxymethyl)benzoylamido>-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / pyridine / CH₂Cl₂ / 16 h / Ambient temperature

2: 55 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 48 h / Ambient temperature

With pyridine; 3 A molecular sieve; iron(III) chloride; In dichloromethane;