1-[(benzylsulfanyl)methyl]-3-nitrobenzene

Base Information

Chemical Name:1-[(benzylsulfanyl)methyl]-3-nitrobenzene
CAS No.:1184780-08-2
Molecular Formula:C₁₄H₁₃NO₂S
Molecular Weight:259.329
Hs Code.:

Synonyms:1-[(benzylsulfanyl)methyl]-3-nitrobenzene

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Chemical Property of 1-[(benzylsulfanyl)methyl]-3-nitrobenzene

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Technology Process of 1-[(benzylsulfanyl)methyl]-3-nitrobenzene

There total 1 articles about 1-[(benzylsulfanyl)methyl]-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1589-82-8
phenylmagnesium bromide

: 619-23-8
3-Nitrobenzyl chloride

: 1184780-08-2
1-[(benzylsulfanyl)methyl]-3-nitrobenzene

Guidance literature:: benzylmagnesium bromide; With sulfur; In tetrahydrofuran; at 50 ℃; for 1h;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 50 ℃;

3-Nitrobenzyl chloride; Further stages;

Reference yield:

: 1184780-08-2
1-[(benzylsulfanyl)methyl]-3-nitrobenzene

: 1-[(benzylsulfonyl)methyl]-3-nitrobenzene

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo3021852

Reference yield:

: 1184780-08-2
1-[(benzylsulfanyl)methyl]-3-nitrobenzene

: 14064-52-9
3-nitrostilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2: 1,2-dibromo-1,1,2,2-tetrachloroethane; alumina-supported potassium hydroxide / tetrahydrofuran; tert-butyl alcohol / 8 h / 20 °C

With 1,2-dibromo-1,1,2,2-tetrachloroethane; alumina-supported potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; tert-butyl alcohol; 2: |Ramberg-Baecklund Rearrangement;
DOI:10.1021/jo3021852