Technology Process of C43H51N7O9
There total 11 articles about C43H51N7O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C44H50N4O11;
With
lithium hydroxide;
In
tetrahydrofuran; water;
at 23 ℃;
for 0.5h;
With
diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate;
In
ethyl acetate;
at 0 - 23 ℃;
Inert atmosphere;
DOI:10.1039/c0cc02214d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C
2.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere
3.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C
3.2: 0 - 23 °C / Inert atmosphere
With
manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
3.2: Mitsunobu reaction;
DOI:10.1039/c0cc02214d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trichlorophosphate / mineral oil / 2 h / 0 - 23 °C / Inert atmosphere
1.2: 1 h / 23 °C / Cooling with ice
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
2.2: 2 h / -78 °C
3.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C
4.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere
5.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C
5.2: 0 - 23 °C / Inert atmosphere
With
manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; lithium hydroxide; lithium hexamethyldisilazane; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; water; mineral oil;
5.2: Mitsunobu reaction;
DOI:10.1039/c0cc02214d
