(4S,8R)-4,8-dimethyldecanal dimethylacetal

Base Information

Chemical Name:(4S,8R)-4,8-dimethyldecanal dimethylacetal
CAS No.:87118-43-2
Molecular Formula:C₁₄H₃₀O₂
Molecular Weight:230.391
Hs Code.:

Synonyms:(4S,8R)-4,8-dimethyldecanal dimethylacetal

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Chemical Property of (4S,8R)-4,8-dimethyldecanal dimethylacetal

Chemical Property:

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Technology Process of (4S,8R)-4,8-dimethyldecanal dimethylacetal

There total 29 articles about (4S,8R)-4,8-dimethyldecanal dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 15681-48-8
lithium dimethylcuprate

: 108864-08-0
Toluene-4-sulfonic acid (2R,6S)-9,9-dimethoxy-2,6-dimethyl-nonyl ester

: 87106-39-6,87118-43-2,97271-12-0,97271-13-1,106445-80-1,108943-54-0
(4R,8R)-1,1-Dimethoxy-4,8-dimethyl-decane

Guidance literature:: In diethyl ether;
DOI:10.1016/S0040-4039(00)85003-0

Reference yield: 59.0%

: 132723-91-2,132830-30-9,132830-31-0,132830-32-1
6-benzenesulfonyl-1,1-dimethoxy-4,8-dimethyldecane

: 87118-43-2
(4S,8R)-4,8-dimethyldecanal dimethylacetal

Guidance literature:: With lithium ethylamide; In tetrahydrofuran; for 1h;

Reference yield:

: 99032-67-4
(S)-(+)-1-bromo-2-methylbutane

: 87118-43-2
(4S,8R)-4,8-dimethyldecanal dimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) hexane, THF, hexamethylphosphoric triamide, -60 deg C, 2.) -60 deg C -> RT, 2.5 h

2: 59 percent / lithium ethylamide / tetrahydrofuran / 1 h

With n-butyllithium; lithium ethylamide; In tetrahydrofuran;