{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

Base Information

Chemical Name:{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel
CAS No.:1426169-47-2
Molecular Formula:C₄₈H₃₀Br₂Cl₂N₂Ni
Molecular Weight:924.184
Hs Code.:

Synonyms:{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

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Chemical Property of {bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

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Technology Process of {bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

There total 8 articles about {bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 1426169-44-9
bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene

: 1426169-47-2
{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

Guidance literature:: In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.molcata.2013.01.016

Reference yield:

: 106-47-8
4-chloro-aniline

: 1426169-47-2
{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

Guidance literature:: Multi-step reaction with 6 steps

1: dichloromethane / 0.5 h / Inert atmosphere

2: bromine / dichloromethane / 5 h / 5 °C / Inert atmosphere

3: sodium hydroxide / dichloromethane; water

4: palladium diacetate; potassium carbonate / 24 h / 25 °C / Inert atmosphere

5: toluene-4-sulfonic acid / benzene / 24 h / Inert atmosphere; Reflux

6: dichloromethane / 24 h / 20 °C / Inert atmosphere

With bromine; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In dichloromethane; water; benzene; 4: |Suzuki Coupling;
DOI:10.1016/j.molcata.2013.01.016

Reference yield:

: 874-17-9
4-chloro-2,6-dibromoaniline

: 1426169-47-2
{bis[N,N'-(4-chloro-2,6-diphenylphenyl)imino]acenaphthene}dibromonickel

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; potassium carbonate / 24 h / 25 °C / Inert atmosphere

2: toluene-4-sulfonic acid / benzene / 24 h / Inert atmosphere; Reflux

3: dichloromethane / 24 h / 20 °C / Inert atmosphere

With palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; In dichloromethane; benzene; 1: |Suzuki Coupling;
DOI:10.1016/j.molcata.2013.01.016