4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

Base Information

Chemical Name:4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride
CAS No.:2182-22-1
Molecular Formula:C₁₃H₁₀FN₃O₆S₂
Molecular Weight:387.369
Hs Code.:

Synonyms:4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

Chemical Property:

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Technology Process of 4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

There total 1 articles about 4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52119-38-7
ethyl 3-oxo-3-(3-nitrophenyl)propanoate

: 2196-72-7
2-Amino-4-methyl-5-fluorsulfonyl-thiazol

: 2182-22-1
4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

Guidance literature:: DOI:10.1021/jo01016a038

Reference yield:

: 2182-22-1
4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

: 2161-73-1
2-[3-(3-amino-phenyl)-3-oxo-propionylamino]-4-methyl-thiazole-5-sulfonyl fluoride

Guidance literature:: With hydrogen; nickel; In 1,4-dioxane; at 80 ℃; under 77572.2 Torr;
DOI:10.1021/jo01016a038

Reference yield:

: 2182-22-1
4-methyl-2-[3-(3-nitro-phenyl)-3-oxo-propionylamino]-thiazole-5-sulfonyl fluoride

: 2161-71-9
2-[3-(3-hexadecanoylamino-phenyl)-3-oxo-propionylamino]-4-methyl-thiazole-5-sulfonyl fluoride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Raney-Ni / dioxane / 80 °C / 77572.2 Torr

2: Py / benzene

With pyridine; hydrogen; nickel; In 1,4-dioxane; benzene;
DOI:10.1021/jo01016a038