Technology Process of dimethylsulfamic acid 5-tert-butyl-4-mercapto-2-methylphenyl ester
There total 5 articles about dimethylsulfamic acid 5-tert-butyl-4-mercapto-2-methylphenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium dihydrogenphosphate; diothiothreitol;
In
ethanol;
Heating;
DOI:10.1021/jm990281p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: H2 / Raney Ni / methanol / 15 h / 35 °C / 2689.24 Torr
2: aq. NaNO2; aq. 15percent H2SO4 / 0.5 h / 70 °C
3: Br2; NaBr / methanol / 0.5 h / 5 - 40 °C
4: 49 percent / Cs2CO3 / acetonitrile / Heating
5: 100 percent / dithiothreitol; 0.02M KH2PO4 / ethanol / Heating
With
potassium dihydrogenphosphate; hydrogen; bromine; caesium carbonate; sodium bromide; sodium nitrite; diothiothreitol;
nickel;
In
methanol; ethanol; acetonitrile;
1: Reduction / 2: Diazotization / 3: Substitution / 4: Sulfonylation / 5: Hydrolysis;
DOI:10.1021/jm990281p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Br2; NaBr / methanol / 0.5 h / 5 - 40 °C
2: 49 percent / Cs2CO3 / acetonitrile / Heating
3: 100 percent / dithiothreitol; 0.02M KH2PO4 / ethanol / Heating
With
potassium dihydrogenphosphate; bromine; caesium carbonate; sodium bromide; diothiothreitol;
In
methanol; ethanol; acetonitrile;
1: Substitution / 2: Sulfonylation / 3: Hydrolysis;
DOI:10.1021/jm990281p
